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This book provides a comprehensive presentation of the most frequently used high resolution manufacturing techniques available, as well as the polymeric materials used for each of the techniques. Divided into two parts covering the technologies and materials used and the impact on different research fields and case studies, High Resolution Manufacturing from 2D to 3D/4D Printing: Applications in Engineering and Medicine addresses issues like throughput improvement by volumetric 3D printing and presenting novel applications and case studies. In addition, this book also covers the latest breakthrough developments and innovations to help readers understand the future applications of this technology across various disciplines, including biomedicine, electronics, energy, and photonics.
Nonlinear Structures & Systems, Volume 1: Proceedings of the 41st IMAC, A Conference and Exposition on Structural Dynamics, 2023, the first volume of ten from the Conference brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on fundamental and applied aspects of Nonlinear Dynamics, including papers on:Experimental Nonlinear DynamicsJointed Structures: Identification, Mechanics, DynamicsNonlinear DampingNonlinear Modeling and SimulationNonlinear Reduced-Order ModelingNonlinearity and System Identification
The book has been designed as a textbook for graduate and postgraduate students of physics, material science, and engineering. This is the third edition of the textbook, that is updated to reflect recent works in the field. In this edition, some new topics have been introduced while some of the existing topics like phonons, Drude -Lorentz model, Fermi levels, electrons, and holes, etc. are modified. Moreover, the book has complete information on semiconductor devices like tunnel diode, Gunn diode, photodiode, photoconductive diode, varactor diode, solar cell, LED, semiconductor lasers, and semiconductor detectors. All the chapters have been supplemented by solved and unsolved examples. Some of the chapters illustrate areas of current interest in solid-state physics to give the student practical working knowledge of the subject text in a simple and lucid manner. There is a fair amount of detail in the examples and derivations given in the text. Each section of the book has exercises to reinforce the concepts, and problems have been added at the end of each chapter. The detailed coverage and pedagogical tools make this an ideal textbook for students and researchers enrolled in graduate and postgraduate courses of physics, material science, and engineering.
This book discusses the extraction, purification, modification, and processing of biobased materials and their various industrial applications, across biomedical, pharmaceutical, construction, and other industries. It includes contributions from experts on hybrid biopolymers and bio-composites, bioactive and biodegradable materials, bio-inert polymers, natural polymers and composites, and metallic natural materials. Therefore, this encyclopedia is a useful reference for scientists, academicians, research scholars, and technologists. Major challenges of biobased materials are their efficient development, cost-effective, and green & environment friendly production/applications. This encyclopedia answers these challenges to professionals and scientists for proper utilization of biobased materials. It presents the recent practices of biobased materials technology in different scientific and engineering domains. It helps the bounded industrial outcomes to reach the general readership of different domains. This encyclopedia bridges the technological gaps between the industrial and academic professionals and the novice young students/scholars. The interdisciplinarity of this encyclopedia makes it unique for a wide readership. The topic of biobased materials is currently popular in the scientific community, working in such following areas as Recycled materials, Renewable materials, Materials for efficiency, Materials for waste treatment, Materials for reduction of environmental load, Materials for easy disposal or recycle, Hazardous free materials, Materials for reducing human health impact, Materials for energy efficiency, Materials for green energy, etc. This is a relatively hot topic in materials science and has strong demands for energy, material and money savings, as well as heavy contamination problems, despite that the area of biobased materials belongs to most important fields of modern science & technology, no important encyclopedias have been published in the area of "e;biobased materials"e;
This book provides a comprehensive overview on the recent significant advancements of conductive polymers and their composites in terms of conductive mechanism, fabrication strategies, important properties, and various promising applications. The corresponding knowledge was systematically compiled in the logical order and demonstrated as seven chapters. The special structure, influencing factors of the conductivity, the charge carrier transport model, the wettability and classical categories of the conductive polymers are narrated. Both conventional and novel strategies undertaken to fabricate the conductive polymers are introduced, as provided the overall master of the progress. In comparison with the bulk counterpart, nanostructured conductive polymers with different dimensions such as nanospheres, nano-networks, nanotubes and nanowire arrays are produced through distinct methods, thus presenting unique and distinct performance endowed by the nanometer scale. The combination of conductive polymers with other functional materials results in a number of the composites with improved properties by synergistic effect. The superior performance of conductive polymers and their composites greatly facilitates their development toward various important applications in the advanced and sophisticated fields such as biological utilization, energy storage and sensors. Due to their excellent biocompatibility, conductive polymers and their composites stand out to be useful in the biological field including tissue engineering, drug delivery and artificial muscle. To meet the urgent demand of the energy storage, conductive polymers and their composites play an important role in the devices including supercapacitors, solar cells and fuel cells. Finally, development of conductive polymers and their composites in the modern industry is greatly enhanced by their applications in smart sensors such as conductometric sensors, gravimetric sensors, optical sensors, chemical sensors and biosensors. This book has significant value for researchers, graduate students, and engineers carrying out the fundamental research or industrial production of conductive polymers and their composites.
This volume gathers select proceedings of the 10th International Conference on Wave Mechanics and Vibrations (WMVC), held in Lisbon, Portugal, on July 4-6, 2022. It covers recent developments and cutting-edge methods in wave mechanics and vibrations applied to a wide range of engineering problems. It presents analytical and computational studies in structural mechanics, seismology and earthquake engineering, mechanical engineering, aeronautics, robotics and nuclear engineering among others. The volume will be of interest for students, researchers, and professionals interested in the wide-ranging applications of wave mechanics and vibrations.
The thesis contains several pioneering results at the intersection of state-of-the-art materials characterization techniques and machine learning. The use of machine learning empowers the information extraction capability of neutron and photon spectroscopies. In particular, new knowledge and new physics insights to aid spectroscopic analysis may hold great promise for next-generation quantum technology. As a prominent example, the so-called proximity effect at topological material interfaces promises to enable spintronics without energy dissipation and quantum computing with fault tolerance, yet the characteristic spectral features to identify the proximity effect have long been elusive. The work presented within permits a fine resolution of its spectroscopic features and a determination of the proximity effect which could aid further experiments with improved interpretability. A few novel machine learning architectures are proposed in this thesis work which leverage the case when the data is scarce and utilize the internal symmetry of the system to improve the training quality. The work sheds light on future pathways to apply machine learning to augment experiments.
This thesis provides the first atomic length-scale observation of the structural transformation (referred to as lattice reconstruction) that occurs in moire superlattices of twisted bilayer transition metal dichalcogenides (TMDs) at low (I < 2Es) twist angles. Such information is essential for the fundamental understanding of how manipulating the rotational twist-angle between two adjacent 2-dimensional crystals subsequently affects their optical and electrical properties.Studies using Scanning transmission electron microscopy (STEM), a powerful tool for atomic-scale imaging, were limited due to the complexity of the (atomically-thin) sample fabrication requirements. This work developed a unique way to selectively cut and re-stack monolayers of TMDs with a controlled rotational twist angle which could then be easily suspended on a TEM grid to meet the needs of the atomically thin sample requirements. The fabrication technique enabled the study of the two common stacking-polytypes including 3R and 2H (using MoS2 and WS2 as the example) as well as their structural evolution with decreasing twist-angle.Atomic-scale studies were followed by a comprehensive investigation of their electronic properties using scanning probe microscopy and electrical transport measurements of the artificially-engineered structures. The electronic structure of two common stacking-polytypes (3R and 2H) were strikingly different, as revealed by conductive atomic force microscopy. Further studies focused on the 3R-stacking polytype to reveal room-temperature out-of-plane ferroelectricity using tools such as kelvin probe force microscopy, scanning electron microscopy and electrical transport measurements. This work highlights that the unique intrinsic properties of TMDs (i.e. semiconductors with strongly light-matter interaction) combined with the additional twisted degree-of-freedom has great potential to create atomically thin transistors/LEDs with built-in memory storage functions and will further aid in the development of the next generation of optoelectronics.
This PhD thesis reports on investigations of several oxide-based materials using advanced infrared and Raman spectroscopy techniques and in combination with external stimuli such as high magnetic or electric field, sptial confinement in thin film heterostructures and the radiation with UV light. This leads to new results in the fields of superconductivity, electronic polarization states and nanoscale phenomena.Among these, the observation of anomalous polar moments is of great relevance for understanding the electric-field-induced metal-to-insulator transistion; and the demonstration that confocal Raman spectroscopy of backfolded acoustic photons in metal-oxide multilayers can be used as a powerful characterization tool for monitoring their interface properties and layer thickness is an important technical development for the engineering of such functional oxide heterostructures.
This book features selected articles based on contributions presented at the 9th International Symposium on Optics and Its Applications (OPTICS-2022) in Yerevan-Ashtarak, Armenia. The annual OPTICS symposium brings together renowned experts from all over the world working in the fields of atomic optics, plasmonics, optics of nanostructures, as well as the optics of condensed matter, and provides a perfect setting for their discussions of the most recent developments in this area.The 9th iteration in this series, dedicated to the 80th birthday of Academician Eduard Kazaryan, focuses on topics dealing with the spectroscopy of real and artificial atoms, linear and nonlinear optical characteristics of quantum wells, and two-dimensional materials. The book highlights recent results of few-particle optical characteristics of artificial atoms in the framework of the exactly solvable Moshinsky model, as well as an electro-optical analog of the magneto-optical Faraday effect. In addition, a detailed study of the nucleation process, its characterization, as well as electronic and optical properties of graded composition quantum dots in the StranskiKrastanov growth mode, is presented.
This book offers an in-depth technical presentation of photography and details about the inner workings of the digital camera, while keeping the artistic principles in mind. Departing from the current stream, the book treats photography as a highly scientific and technical subject, and serves as a reference to those who seek for an understanding of the technical aspects relating to the photographic camera, the beating heart of photography. It offers insight on why the photographs are created the way they are, highlighting also the limitations. As the author of this book is an image technology scientist and a photography enthusiast who has been teaching photography for a long time, this treatise reflects his own constant search and study for an in-depth understanding.
This book is a platform to publish new progress in the field of materials and technologies that can offer significant developments with the possibility of changing the future. These emerging developments will change the way we live now at an unprecedented pace across our society. It is important to note that such modern developments are no longer restricted to a single discipline, but are the outcome of a multidisciplinary approach, which combines many different engineering disciplines. This book explores the new technology landscape that will have the direct impact on production-related sectors, individually and in combination with different disciplines. A major driver for this actual research is the efficiency, many times connected with a focus on environmental sustainability.
This book provides an accessible overview of the historical background of the chemistry of flexible metal-organic frameworks (MOFs) and their features.
This volume explores the latest advancements and techniques used to study cell analysis, their capabilities, and the type of results that can be obtained. The chapters in this book cover topics such as FACS; fluorescence microscopy; organic spectroscopy such as MALDI; inorganic spectroscopy such as ICP-MS; and sequencing. Written in the highly successful Methods in Molecular Biology series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and tips on troubleshooting and avoiding known pitfalls.Cutting-edge and practical, Single Cell Analysis: Methods and Protocols is a valuable tool for any researcher interested in learning more about this important and developing field.
Sustainable Fillers/Plasticizers for Polymer Composites: Promising Resources presents a comprehensive review of the application and use of biofillers and bioplasticizers for the fabrication of biopolymer-based composites. This book looks first at the historical aspects and then goes on to discuss current trends and recent developments. Emphasis is placed on the future potential of these resources to expand their usage in a broad range of different applications. This book will be a valuable reference resource for both academic and industrial researchers working in materials science, polymer chemistry and engineering, and the manufacturing of polymer composite materials.
Advanced Materials for Battery Separators focuses solely on battery separators and their significance, providing the reader with a detailed description of their use in both aqueous and non-aqueous batteries. Topics include separator requirements and classifications, as well as discussions of the different methods for the fabrication of separators, experimental techniques used for the characterization of separators, and their physical and chemical properties. It concludes with a look at the challenges and new technologies developed to improve the performance of separators. This book is a valuable reference for engineers, research scholars, and for graduates and post graduates primarily in the field of material science, electrochemistry, and polymer chemistry. It can also be useful for engineers and technologists working in both industry and the energy field.
This book gives an insight into the current developments in the field of continuum mechanics. Twenty-five researchers present new theoretical concepts, e.g., better inclusion of the microstructure in the models describing material behavior. At the same time, there are also more applications for the theories in engineering practice.In addition to new theoretical approaches in continuum mechanics and applications, the book puts an emphasis on discussing multi-physics problems.
The book is intended for practicing engineers in the oil industry, researchers, and graduate students interested in designing and simulating offshore hydrocarbon production systems. It approaches offshore oil production systems from an integrated perspective that combines the modeling of thermophysical properties of reservoir fluids and their flow as a multiphase mixture in wellbores, flow lines, and risers.The first part of the book presents an internally consistent method to compute the critical parameters and acentric factor of Single Carbon Number (SCN) fractions of petroleum mixtures using state-of-the-art multivariate fitting techniques. The procedure is illustrated and validated using flash and differential liberation data from actual field samples. In the second part of the book, mechanistic multiphase flow models are discussed in light of their ability to predict the pressure, temperature, and phase holdup of production fluids in wellbores, flow lines, and risers. Multivariate fitting procedures are again applied to evaluate the sensitivity of the results with respect to closure relationship parameters, such as slug body gas holdup, wall shear stress, and wall roughness in pipelines and production tubing. Finally, the modeling framework is validated using actual field data from offshore production wells.
This contributed volume provides a critical review of research in the field of Electrochemical Promotion of Catalysis (EPOC). It presents recent developments during the past decade that have led to a better understanding of the field and towards applications of the EPOC concept. The chapters focus on the implementation of EPOC for developing sinter-resistant catalysts, catalysts for hydrogen production, ammonia production and carbon dioxide valorization. The book also highlights the developments towards electropromoted dispersed catalysts and for self-sustained electrochemical promotion which are currently expanding. This authoritative analysis of EPOC is useful for various scientific communities working at the interface of heterogeneous catalysis, solid state electrochemistry and materials science. It is of particular interest to groups whose research focuses on developments towards a better and more sustainable future.
This book looks at chemmotological solutions to important questions surrounding sustainability and environmental safety of transport - both key priorities within the global strategy of sustainable development. Bringing together expanded versions of selected papers presented at the 8th International Scientific-Technical Conference: Problems of Chemmotology - Theory and Practice of Rational Use of Conventional and Alternative Fuels and Lubricants, contributors present solutions to problematic questions, including choosing feedstock and technologies of its processing for manufacturing alternative fuels, development and implementation of measures for improving environmental safety of transport, minimizing exhaust gases emission from transport, introducing new solution or improvements in systems of fuels supply and infrastructure, and changes in legislative and regulatory base for fuels and lubricants use. This collection will be an invaluable reference for researchers, professionals, and students involved in alternative aviation fuels, transport engineering, sustainable transport development, and fuels and lubricants.
This textbook has been written for the engineering students. This textbook covers the essentials of solid mechanics with reference to basic load-bearing members¿straight bars, thin-walled cylindrical and spherical pressure vessels, circular shafts, beams undergoing simple bending, and columns. It concisely elucidates the corresponding fundamental assumptions, important equations, and their range of validity without formal derivations. Subsequently, this textbook contains several carefully selected examples to illustrate sequence of steps in the analysis of forces, stresses and displacements, or stability. It further deals with combined loading, stress and strain transformations, energy methods, and failure analysis using commonly employed criteria. This textbook is a handy, yet complete, resource for graduate and postgraduate engineering students. It will also be a ready reference for a practicing engineers or graduate students preparing for an interview or a competitive examination.
This thesis describes in-depth studies of the remarkable electronic transport within the ultrahigh conductivity delafossite metals PtCoO_2 and PdCoO_2 using the tool of focused ion beam (FIB) microstucturing. Despite being first synthesised over 50 years ago, important questions remain regarding both the origin of the unusually high conductivity of these compounds and the consequences of their unique properties for unconventional electronic transport, such as that within the ballistic regime. The thesis explores both these areas.High-energy electron irradiation is used to examine the effects of deliberately introducing point defects into PdCoO_2 and PtCoO_2, demonstrating that the extremely low resistivity of these materials stems from an extreme purity as high as 1 defect in 120,000 atoms, rather than a novel scattering suppression mechanism. In addition, studies of the electronic transport in micron-scale squares of these metals show that their broadly hexagonal Fermi surfaces lead not only to long range ballistic behaviour but novel ballistic regime phenomena which cannot be observed in materials with a higher-symmetry Fermi surface.
Additive manufacturing classification is one of the biggest issues faced by AM community. The book provides a comprehensive classification of AM, which can be useful to anyone working in any area of manufacturing. As the classification depends on the interrelation of various AM processes, the book provides concise and critical information of those processes, which can be helpful to anyone looking for a concise book on AM. The book provides original information unavailable in research papers.
This book looks at the recent developments in the area of photocatalytic degradation of dyes using photocatalytic techniques, for example by means of various nanoparticles, heterogeneous, and hybrid systems. Dyes are one of the major groups of water pollutants and are widely used in a diverse range of industries. The toxic effects of organic dyes in wastewater can have a great environmental impact, therefore there is significant interest and need to remove these dyes effectively and efficiently during wastewater treatment.This volume covers a plethora of basics on the photochemistry of dyes and provides information on technological perspectives including reactor designs and process intensification. Since many industries release a significant amount of colored effluents, which are toxic and difficult to remove by conventional methods, the comprehensive studies herein will contribute to helping reduce the impact of colored effluents in wastewater on the environment.
This book elucidates the peculiar phenomenon of entropy/enthalpy compensation that takes place in high performance liquid chromatography (HPLC) of polymers. Numerous publications, including some books, are devoted to molecular characterization of synthetic polymers, materials presently produced in large and steadily growing quantities, applying methods of HPLC. A knowledge of the molecular characteristics of polymers is indispensable, not only for their proper applications but also for their recycling and remediation. Polymer scientists generally focus on synthesis and potential applications of polymers while not giving due attention to an important central link, their comprehensive characterization in context of development of structure-property correlations. To fill this gap is one of the aims of the present book. The process of entropy/enthalpy compensation plays a decisive role in the advanced method of polymer characterization such as liquid chromatography at critical conditions, eluent gradient interaction chromatography, and temperature gradient interaction chromatography. All chemists working on any aspect of polymer science will find this book a valuable resource for the development of structure-property correlations.
This book covers synthesis, characterization, and applications of diverse types of nanomaterials. Specifically, it describes carbon, graphene, and graphene oxide-based nanomaterials and their use for environmental remediation; rare-earth ions-activated nanophosphors and their application; lanthanide-based oxides as advanced nanostructured materials for organic decontamination; and advanced functional nanomaterials for pollutant sensing and water remediation. The chapters explore the use of nanomaterials in solid-phase extraction technique, design of colorimetric sensor based on gold nanoparticles, optical sources and waveguides based on flexible 1D nanomaterials, synthesis and property characterization of 2D materials with applications, and the scale effects on the value of the surface energy of a solid. The developments of some nanomaterials such as zinc and nickel sulfides as photocatalysts and electrocatalysts, effects of reducing size and incorporation of nanoadditives, advanced carbon nanomaterials such as carbon nanotubes, carbon nanofibers, and graphene and its derivations as adsorbents, and carbon spheres and carbon soot for tribological applications are also presented in this book. In addition, nanomaterials for concrete coating applications and advances in the processing of high-entropy alloys by means of mechanical alloying are also covered. Subsequently, the use of nanomaterials in endodontics and the use of nanotechnology strategies to enhance restorative resin-based dental nanomaterials are reported.
This book provides a selection of recent developments in scanning ion conductance microscopy (SICM) technology and applications. In recent years, SICM has been applied in an ever-increasing number of areas in the bioanalytical sciences. SICM is based on an electrolyte-filled nanopipette with a nanometer-scale opening, over which an electric potential is applied. The induced ion current is measured, which allows to directly or indirectly quantify various physical quantities such as pipette-sample distance, ion concentration, sample elastic modulus among many others. This makes SICM well suited for applications in electrolytes - most prominently for the study of live cells.This book starts with a historic overview starting from the days of the invention of SICM by Paul Hansma at the University of California at Santa Barbara in 1989. SICM is a member of the family of scanning probe microscopies. It is related to another prominent member of the family, atomic force microscopy (AFM), which has found application in almost any field of nanoscale science. The advantages and disadvantages of SICM over AFM are also outlined. One of the most effective and break-through applications of SICM nanopipettes is in electrochemistry. The different routes and applications for doing electrochemistry using nanopipettes are also discussed. In addition the book highlights the ability of SICM for surface positioning with nanometer precision to open up new vistas in patch clamp measurements subcellular structures. Finally the book presents one research area where SICM has been making a lot of contributions, cardiac research and the endeavors to combine SICM with super-resolution optical microscopy for highest-resolution joint topography and functional imaging.
This book provides a detailed, self-contained description of automatic indexing of crystal diffraction patterns, considering both ab initio indexing and indexing of patterns originating from known structures. Introductory chapters equip the reader with the necessary basic knowledge of geometric crystallography, as well as kinematic and dynamic theories of crystal diffraction. Subsequent chapters delve and describe ab initio indexing of single crystal diffraction patterns and indexing of patterns for orientation determination. The book also reviews methods of indexing powder diffraction and electron spot-type patterns, as well the subject of multigrain indexing. Later chapters are devoted to diffraction by helical structures and quasicrystals, as well as some aspects of lattice parameter refinement and strain determination.The book is intended equally for materials scientists curious about 'nuts and bolts' of diffraction pattern indexing and orientation mapping systems, as well as interdisciplinary researchers from physics, chemistry, and biology involved in crystallographic computing. It provides a rigorous, yet accessible, treatment of the subject matter for graduate students interested in understanding the functioning of diffraction pattern indexing engines.
This volume provides a wide spectrum of multidisciplinary approaches for studying RNA structure and dynamics, including detailed accounts of experimental and computational procedures. Chapters guide readers through cryo-electron microscopy, crystallography, isothermal titration calorimetry, small angle X-ray scattering, single-molecule Forster Energy transfer, X-ray free electron laser, atomic force microscopy, computational simulation, and prediction. Written in the format of the highly successful Methods in Molecular Biology series, each chapter includes an introduction to the topic, lists necessary materials and reagents, includes tips on troubleshooting and known pitfalls, and step-by-step, readily reproducible protocols.Authoritative and cutting-edge, RNA Structure and Dynamics aims to be a foundation for future studies and to be a source of inspiration for new investigations in the field.
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